|
see also:
Algorithm of Kinetic
Analysis,
Applications,
The basis of analysis are
measurements, executed with the methods:
thermogravimetry (TGA),
differential scanning calorimetry (DSC, DTA),
mass spectrometry (MS),
dilatometry (DIL),
rheometry and its special variant vulcametry (RHEO, VULC).
The general interface to measurement data are ASCII
files
In the program
Thermokinetics are integrated various methods of kinetic
analysis and of predictions as well as
Model-free Kinetic
Analysis
Friedman analysis of dynamic and/or isothermal
measurements
Ozawa-Flynn-Wall analysis of dynamic measurements
Analysis according ASTM E698
Model-fit using
Multivariate Nonlinear Regression
|

|
Model definition,
including multiple step reactions and 18 different
reaction types
Conditions for parameters
|
|

|
Visual
optimization in order to achieve a good start
position for the nonlinear
regression
|
|

|
Nonlinear
regression. Conditions of iteration. Results
are:
- optimized parameters including standard
errors
- F-test regarding the fit quality
- F-test regarding significance of an additional
step
- Graphic presentation
|
Isothermal Prediction
and Prediction on the Base of a User Defined
Temperature Program
|

|
Isothermal
prediction of signal
Dynamic prediction of signal
|
|

|
Tabular report of
signal and degree of reaction versus time for a set
of temperatures
|
|

|
Isothermal
prediction of degree of reaction
Dynamic prediction of degree of reaction
|
|

|
Isothermal
prediction of formal reactants
Dynamic prediction of formal reactants
|
|